Perchloric acid: Difference between revisions
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===Extraction=== | ===Extraction=== | ||
===Synthesis=== | ===Synthesis=== | ||
====from a saturated sodium perchlorate solution==== | |||
{{#Chem: NaClO4(aq) + HCl(aq) → NaCl(s) + HClO4}} | |||
====also==== | |||
*{{cite pub | *{{cite pub | ||
|publication= J. Am. Chem. Soc. | |publication= J. Am. Chem. Soc. | ||
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|url=https://pubs.acs.org/doi/pdf/10.1021/ja02212a006}} | |url=https://pubs.acs.org/doi/pdf/10.1021/ja02212a006}} | ||
*Combine [[hydrochloric acid]], [[nitric acid]], and [[ammonium perchlorate]]<ref>{{cite web|url=https://www.youtube.com/watch?v=rUFsvlsi08E&t=554s | *Combine [[hydrochloric acid]], [[nitric acid]], and aqueous [[ammonium perchlorate]]<ref>{{cite web|url=https://www.youtube.com/watch?v=rUFsvlsi08E&t=554s | ||
|title=Making Perchloric Acid (no dangerous fumes!)}}</ref><ref>{{cite web|url=https://www.youtube.com/watch?v=wNN_MCr_mrA&t=34s|title= Perchloric Acid-HClO4 }}</ref> | |title=Making Perchloric Acid (no dangerous fumes!)}}</ref><ref>{{cite web|url=https://www.youtube.com/watch?v=wNN_MCr_mrA&t=34s|title= Perchloric Acid-HClO4 }}</ref> | ||
:{{#Chem:9HCl + 36HNO3 +34NH4ClO4(aq) = 34 HClO4 + 4Cl2 + 35N2O+ 73H2O}} | :{{#Chem:9HCl + 36HNO3 +34NH4ClO4(aq) = 34 HClO4 + 4Cl2 + 35N2O+ 73H2O}} |
Latest revision as of 00:37, 3 December 2024
Chemical formula | HClO4 |
---|---|
OTP appearance | clear liquid |
Molar Mass(g/mol) | 100.46 |
Density(g/cc) | 1.768 |
Melting Point(°C) | -17 |
Boiling Point(°C) | 203 |
Solubility in water(g/L) | misc |
NFPA 704 |
Uses
Justification Questioned
Other
Natural occurrence
Hazards
Character
Production
Extraction
Synthesis
from a saturated sodium perchlorate solution
NaClO4(aq) + HCl(aq) → NaCl(s) + HClO4
also
- (1912) "THE PREPARATION OF PERCHLORIC ACID" (local copy)
J. Am. Chem. Soc. 34(11)
DOI:10.1021/ja02212a006
- Combine hydrochloric acid, nitric acid, and aqueous ammonium perchlorate[1][2]
- 9 HCl + 36 HNO3 + 34 NH4ClO4(aq) → 34 HClO4 + 4 Cl2 + 35 N2O + 73 H2O