Perchloric acid: Difference between revisions
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===Extraction=== | ===Extraction=== | ||
===Synthesis=== | ===Synthesis=== | ||
*{{cite pub | |||
|publication= J. Am. Chem. Soc. | |||
|year=1912 | |||
|volume=34 | |||
|issue=11 | |||
|pp=1480–1485 | |||
|title=THE PREPARATION OF PERCHLORIC ACID | |||
|doi=10.1021/ja02212a006 | |||
|url=https://pubs.acs.org/doi/pdf/10.1021/ja02212a006}} | |||
Combine [[hydrochloric acid]], [[nitric acid]], and [[ammonium perchlorate]]<ref>{{cite web|url=https://www.youtube.com/watch?v=rUFsvlsi08E&t=554s | *Combine [[hydrochloric acid]], [[nitric acid]], and [[ammonium perchlorate]]<ref>{{cite web|url=https://www.youtube.com/watch?v=rUFsvlsi08E&t=554s | ||
|title=Making Perchloric Acid (no dangerous fumes!)}}</ref><ref>{{cite web|url=https://www.youtube.com/watch?v=wNN_MCr_mrA&t=34s|title= Perchloric Acid-HClO4 }}</ref> | |title=Making Perchloric Acid (no dangerous fumes!)}}</ref><ref>{{cite web|url=https://www.youtube.com/watch?v=wNN_MCr_mrA&t=34s|title= Perchloric Acid-HClO4 }}</ref> | ||
:{{#Chem:9HCl + 36HNO3 +34NH4ClO4(aq) = 34 HClO4 + 4Cl2 + 35N2O+ 73H2O}} | :{{#Chem:9HCl + 36HNO3 +34NH4ClO4(aq) = 34 HClO4 + 4Cl2 + 35N2O+ 73H2O}} | ||
Revision as of 20:40, 11 October 2023
| Chemical formula | HClO4 |
|---|---|
| OTP appearance | clear liquid |
| Molar Mass(g/mol) | 100.46 |
| Density(g/cc) | 1.768 |
| Melting Point(°C) | -17 |
| Boiling Point(°C) | 203 |
| Solubility in water(g/L) | misc |
| NFPA 704 |  0
3
3
OX
|
Uses
Justification Questioned
Other
Natural occurrence
Hazards
Character
Production
Extraction
Synthesis
- (1912) "THE PREPARATION OF PERCHLORIC ACID"
J. Am. Chem. Soc. 34(11)
DOI:10.1021/ja02212a006
- Combine hydrochloric acid, nitric acid, and ammonium perchlorate[1][2]
- 9 HCl + 36 HNO3 + 34 NH4ClO4(aq) → 34 HClO4 + 4 Cl2 + 35 N2O + 73 H2O